1. Pali makhiristo apamwamba kwambiri mu cell conductivity.
Yankho: Mukatsuka ma conductivity cell ndi 1: 1 nitric acid, muzimutsuka ndi madzi a deionized.
2. Chodziwikiratu sichoyera mokwanira.
Chidziwitso: kusintha mawonekedwe.
3. Mzere wa chromatographic umatenga zinthu zamphamvu kwambiri.
Yankho: Washcolumn mobwerezabwereza komanso mosinthana ndi zowoneka bwino ndi madzi.
4. Kusankha molakwika sikelo yoyezera
Pochita kusanthula kwa ma ion, popeza ma conductivity akumbuyo a eluate ndi okwera kwambiri, kusankha kwa sikelo yotsika kwambiri kudzatsogolera ku chiwonetsero chapamwamba kwambiri.Ingosankhanso sikelo yoyezera.
5. Wopondereza sakugwira ntchito
Yankho: Onani ngati chopondereza chayatsidwa.
6. Kuyika kwachitsanzo ndikokwera kwambiri.
Yankho: Chepetsani chitsanzo.
1. Mu mpope muli thovu.
Yankho: valavu yotulutsa motsatana motsatana ndi nthawi yapampu yotulutsa mpweya, mavuvu otopetsa.
2. Valve yowunikira ya mpope yawonongeka kapena yowonongeka.
Yankho: Sinthani valavu ya cheki kapena ikani mu 1: 1 nitric solution poyeretsa kwambiri.
3. Sefa yomwe ili mu botolo lodziwikiratu ili ndi kachilombo kapena kutsekedwa.
Yankho: Bwezerani chosefera.
4. Kusakwanira kutsuka kwa mpweya.
Yankho: Bwezerani chosowa.
Yankho: Yang'anani malo otsekera m'mbali mwa njira yolowera kuti muwone ndikuchotsa kutsekeka.
1. Nembanemba yosefera mzati yatsekedwa.
Yankho: Chotsani ndime ndikuchotsa kumapeto kwa cholowera.Chotsani mbale ya sieve mosamala, ikani mu 1: 1 nitric acid ndikutsuka ndi akupanga yoweyula kwa mphindi 30, ndiye muzimutsuka ndi madzi a deionized ndi kusonkhanitsa izo mmbuyo, n'zosiyana kusonkhanitsa chromatograph kwa rinsing.Dziwani kuti chromatograph singalumikizidwe ndi njira yoyenda.
2. Vavu ya jekeseni wa njira zisanu ndi imodzi yatsekedwa.
Yankho: Yang'anani malo otsekera m'mbali mwa njira yolowera kuti muzindikire ndikuthetsa.
3. Valovu ya cheki ya mpope yatsekedwa.
Yankho: Sinthani valavu ya cheki kapena ikani mu 1: 1 nitric solution poyeretsa kwambiri.
4. Njira yoyenda yatsekedwa.
Yankho: pezani malo otsekera molingana ndi njira yochotsera pang'onopang'ono ndikusinthanso.
5. Kuthamanga kwambiri.
Yankho: Sinthani mpope kuti muyende bwino.
6. Kuthamanga kwa malire a pampu kumayikidwa kwambiri.
Yankho: Pansi pa kayendetsedwe ka ntchito ya chromatographic column, sinthani kukakamiza kwa malire kuti akhale 5 MPa pamwamba pa mphamvu yomwe ikugwira ntchito pano.
1. Chipangizocho sichithamanga kwa nthawi yaitali monga momwe anakonzera.
Yankho: Kulowetsedwa kosalekeza kwa zowoneka mpaka zida zitakhazikika.
2. Pali thovu mu mpope.
Yankho: valavu yotulutsa motsatana motsatana ndi nthawi yapampu yotulutsa mpweya, mavuvu otopetsa.
3. Fyuluta ya chitoliro cholowetsa madzi cha mpope imatsekedwa, kutulutsa kupanikizika koipa pansi pa mphamvu yokoka ndi kutulutsa thovu.
Yankho: M'malo fyuluta kapena kuwayika fyuluta mu 1:1 1M nitric asidi kutsukidwa 5min ndi akupanga kusamba.
4. Pali thovu muzambiri.
Yankho: Gwiritsani ntchito zomwe zakonzedwa ndi madzi oyeretsedwa kuti mutsuka ndimeyo mofulumira kuti muchotse thovu.
5. Pali thovu mu njira yoyenda.
Yankho: Chotsani mzati ndikutulutsa thovu m'madzi.
6. Pali thovu mu conductivity selo, zomwe zimayambitsa kusinthasintha wokhazikika wa zoyambira.
Yankho: Flushing conductivity cel, thovu lotopetsa
7. Voltage ndi yosakhazikika kapena kusokonezedwa ndi static electrostatic.
Yankho: Onjezani chowonjezera chamagetsi ndikutsitsa chidacho.
1. Nthawi yowotchera isanayambe ya chipangizocho ndi yosakwanira.
Yankho: Wonjezerani nthawi yotentha isanayambe.
2. Kutaya kutayikira.
Yankho: fufuzani malo omwe akutayikira ndikuwongolera, ngati sangathe kuthetsedwa, sinthani olowa.
3. Voltage ndi yosakhazikika kapena kusokonezedwa ndi static electrostatic.
Yankho: Onjezani chowonjezera chamagetsi ndikutsitsa chidacho.
1. Kuchulukirachulukira kwa osadziwika sikoyenera.
Anakonza: Sankhani yoyenera ndende .
2. Kuthamanga kwa eluentis kukukwera kwambiri.
Yankho: Sankhani liwiro loyenda bwino la osowa.
3. Kugwiritsa ntchito zitsanzo zokhala ndi chidwi kwambiri
Yankho: Chepetsani chitsanzo.
4. Mzerewu waipitsidwa .
Yankho: Bweretsaninso kapena kusintha gawolo.
1. Kuchuluka kwa jekeseni wa chitsanzo sichiri nthawi zonse.
Yankho: Jayini zitsanzo pa voliyumu yopitilira ka 10 kuchuluka kwa mphete kuti mutsimikizire jekeseni yonse.
2. Kuchuluka kwa jekeseni wojambulidwa ndi kosayenera.
Yankho: Sankhani jekeseni yoyenera ya chitsanzo.
3. The reagent ndi yodetsedwa.
Yankho: Bwezerani m'malo mwa reagent.
4. Zinthu zachilendo zimapezeka m'madzi osungunuka.
Yankho: Bwezerani madzi osungunuka.
5. Kuthamanga kumasintha.
Yankho: Pezani zifukwa zakusintha koteroko ndikusintha kuti zikhale momwe zinalili poyamba.
6. Njira yothamanga yatsekedwa.
Yankho: pezani malo otsekedwa, konzani kapena sinthani.
1. The reagent si yoyera.
Yankho: Bwezerani ma reagents.
2. Madzi osakanizidwa amakhala ndi zonyansa.
Yankho: Bwezerani madzi osungunuka.
1. Kuyika kolakwika kwa cell conductivity.
Yankho: Ikaninso cell conductivity.
2. Conductivity madutsidwe selo kuonongeka.
Yankho: Bwezerani cell conductivity.
3. Pampu ilibe yankho lotulutsa.
Yankho: Yang'anani chizindikiro cha kuthamanga kuti muwone ngati mpope ikugwira ntchito.
1. Njira yothetsera vutoli ndi yoipitsidwa, makamaka zitsanzo zotsika kwambiri.
Yankho: Konzaninso yankho.
2. Madzi osakanizidwa ndi odetsedwa.
Yankho: m'malo mwa madzi a deionized.
3. Kuchulukitsitsa kwachitsanzo ndikokwera kwambiri kapena kutsika kwambiri, kunja kwa mzere wa chipangizocho.
Yankho: Sankhani yoyenera ndende.
Yankho: sinthani chingwe chamagetsi kapena magetsi osasintha.
1. Gasi wolowetsedwa mumsewu wopita
Yankho: madzi akayatsidwa, tsegulani valavu ya mpope, yambitsani pampu ya plunger ndikugwedeza fyulutayo kuti muchotse kwathunthu mpweya.
2. Kutentha kwambiri kwa m'nyumba kumapangitsa kuti madzi asungunuke osakwanira.
Yankho: Gwiritsani ntchito chipangizo chochotsera gasi pa intaneti.
3. Valve yowunikira ya mpope yawonongeka kapena yowonongeka.
Yankho: Sinthani valavu ya cheki kapena ikani mu 1: 1 nitric solution poyeretsa kwambiri.